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FEI Titan 80-300 STEM (Titan S)

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DETECTOR
Peltier-cooled Ultrascan 2k charge coupled device (CCD) camera. (Gatan) Tridiem 865 ER image filter (GIF) with fully 2nd and 3rd order and partially 4th order corrected prisms and a maximum field of view of 17 µm for imaging and 120 mR for diffraction analyses, with additional STEM detectors implemented. (Gatan) Model 3000 HAADF detector. (Fischione)

The FEI Titan 80-300 STEM is a scanning transmission electron microscope equipped with a field emission electron gun, a three-condenser lens system, a monochromator unit, and a Cs probe corrector (CEOS), a post-column energy filter system (Gatan Tridiem 865 ER) as well as a Gatan 2k slow scan CCD system. Characterised by a STEM resolution of 80 pm at 300 kV, the instrument was one of the first of a small number of sub-ångström resolution scanning transmission electron microscopes in the world when commissioned in 2006.
Typical Applications and Limitations of Use

The FEI Titan 80-300 STEM allows a variety of advanced scanning transmission electron microscopy investigations to a wide range of materials. Techniques like electron energy loss spectroscopy (EELS), energy filtered transmission electron microscopy (EFTEM), high resolution scanning transmission electron microscopy (HRSTEM) with detectors for bright-field, annular dark-field, and high-angle annular dark field (HAADF) imaging, electron tomography (ET), and combinations of the previous techniques.

The FEI Titan 80-300 STEM is not intended for the investigation of aqueous, contaminated, ferromagnetic or organic samples without further discussions with both of the instruments officers and the ER-C general management.
Sample Environment

Apart from the special case of the utilisation of dedicated cooling or heating stages, the FEI Titan 80-300 STEM will allow samples to be investigated either under room temperature or liquid nitrogen cooling conditions at a vacuum level of about 10–8 mbar. Besides this standard setup, the sample environment can be adapted to various conditions, e.g. thermal treatment under vacuum or under gas atmosphere up to 1 bar using a MEMS-based closed-cell holder, or the application of external electric or magnetic fields to samples, making use of a wide portfolio of in situ TEM holders available at the ER-C.


Publications

Understanding and Controlling Nanoporosity Formation for Improving the Stability of Bimetallic Fuel Cell Catalysts

Gan L, Heggen M, O’Malley R, Theobald B, Strasser P - Nano Letters - 2013


Compositional segregation in shaped Pt alloy nanoparticles and their structural behaviour during electrocatalysis

Cui C, Gan L, Heggen M, Rudi S, Strasser P - Nature Materials - 2013


Core–Shell Compositional Fine Structures of Dealloyed PtxNi1–x Nanoparticles and Their Impact on Oxygen Reduction Catalysis

Gan L, Heggen M, Rudi S, Strasser P - Nano Letters - 2012


Plastic-deformation mechanism in complex solids

Heggen M, Houben L, Feuerbacher M - Nature Materials - 2010


Access
The ER-C provides both, direct services and scientific assistance to university research groups and research laboratories in industry and academia in the field of advanced electron microscopic applications. The support of students is also an integral part of our activities.

Link: https://er-c.org/index.php/access/
FEI Titan 80-300 STEM Image

Helmholtz Imaging spinning wheel

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